Lab Materials

Metallole Synthesis

Fall 2009

 Documents, Instructions, and Useful Websites

Housekeeping Duties & Assignments

Syllabus

USM Laboratory Safety Plan

 Manufacturers' Safety Data Sheets (MSDS)

Resources for Finding Infomation
Introduction to Molecular Modeling

Thin Layer Chromatography
Animated Infrared Spsctroscopy

An Animated NMR Course

An On-Line MS Animation

An On-Line GC-MS Tutorial

DATA BASE OF SPECTRA
SDBS: Integrated Spectral Data Base System for Organic Compounds

Laboratory Handouts: Prudenté

Project Overview
Schedule

Unit

 Introduction
Pre-laboratory Exercises
 Post-laboratory Report
1

X

X

X
2 X X

X
3

X

X

X
4

X

X

X
5 and 6

X

X

 X
SciFinder X --- X

Directions for Final Report

Sample Formal Report

Lab and Instrument Instructions (others coming soon)
(Microsoft Word Documents)

Device

Instructions
IR
X
NMR
X
GC-MS
X
Glove Box
X
TLC
X
Column Chromatography
X
Rotoevaporation
X

Fluorescence Spectroscopy
X (revised 4/18/02)

Interactive NMR Spectra*

Compound
Benzyltriphenylphosphonium bromide
E-stilbene
meso-Stilbenedibromide
Diphenylacetylene

* In order to view these spectra you must have a program called H-NMR Viewer installed on your computer.  This program is available for free from ACD Labs.