Lab Materials

Metallole Synthesis

2008-2009

 Documents, Instructions, and Useful Websites

Syllabus

USM Laboratory Safety Plan

 Manufacturers' Safety Data Sheets (MSDS)

Resources for Finding Infomation

Introduction to Molecular Modeling I 

Thin Layer Chromatography

An Animated NMR Course

An On-Line MS Animation

An On-Line GC-MS Tutorial

DATA BASE OF SPECTRA
SDBS: Integrated Spectral Data Base System for Organic Compounds

Laboratory Handouts: Tracy

Project Overview
Schedule Spring 2009

Unit

 Introduction
Pre-laboratory Exercises
 Post-laboratory Report Post-Laboratory
Report
1

X

X

X

 X
2 X X

X

 X
3

X

X

X

 X
4

X

X

X

 X
5 and 6

X

X

 X X
SciFinder X --- X X

Directions for Final Report

Sample Formal Report

Lab and Instrument Instructions (others coming soon)
(Microsoft Word Documents)

Device

Instructions
IR
X
NMR
X
GC-MS
X
Glove Box
X
TLC
X
Column Chromatography
X
Rotoevaporation
X

Fluorescence Spectroscopy
X (revised 4/18/02)

Interactive NMR Spectra*

Compound
Benzyltriphenylphosphonium bromide
E-stilbene
meso-Stilbenedibromide
Diphenylacetylene

* In order to view these spectra you must have a program called H-NMR Viewer installed on your computer.  This program is available for free from ACD Labs.