Lab Materials

2007-2008

 Documents, Instructions, and Useful Websites

USM Laboratory Safety Plan

 Manufacturers' Safety Data Sheets (MSDS)

Resources for Finding Infomation

Introduction to Molecular Modeling I 

Thin Layer Chromatography

An Animated NMR Course

An On-Line MS Animation

An On-Line GC-MS Tutorial

The Aldrich Catalog

DATA BASE OF SPECTRA
SDBS: Integrated Spectral Data Base System for Organic Compounds

Lab Handouts: Prudenté

Project Overview

Schedule

Experiment

Introduction

Pre-laboratory Exercises

Post-laboratory Report
SciFinder

X

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X

Claisen-Schmidt Reaction X X

X

Bromination of Chalcone X X X
Aziridination X X X

Directions for Final Report

Sample Formal Report

Lab and Instrument Instructions
(Microsoft Word Documents)

Device

Instructions

IR
X
NMR

X

GC-MS

X

TLC
X
Column Chromatography
X
Rotoevaporation
X

Interactive NMR Spectra*

Compound

1H-NMR 13C-NMR
acetophenone acetophenone
chalcone chalcone
chalcone dibromide chalcone dibromide
2-phenyl-3-benzoylaziridine 2-phenyl-3-benzoylaziridine

* In order to view these spectra you must have a program called H-NMR Viewer installed on your computer.  This program is available for free from ACD Labs.