Lab Materials

2006-2007

 Documents, Instructions, and Useful Websites

Syllabus

Schedule

USM Laboratory Safety Plan

 Manufacturers' Safety Data Sheets (MSDS)

Resources for Finding Infomation

Introduction to Molecular Modeling I 

Thin Layer Chromatography

An Animated NMR Course

An On-Line MS Animation

An On-Line GC-MS Tutorial

The Aldrich Catalog

DATA BASE OF SPECTRA
SDBS: Integrated Spectral Data Base System for Organic Compounds

Lab Handouts

Project Overview

Unit

 Introduction

Pre-laboratory Exercises

 Post-laboratory Report
1

X

X

X
2 X X

X
3

X

X

X
4

X

X

X
5 and 6

X

X

 X
SciFinder X --- X
Unknowns X --- X

Directions for Final Report

Sample Formal Report

Lab and Instrument Instructions
(Microsoft Word Documents)

Device

Instructions
IR
X
NMR

X
GC-MS

X
Glove Box
X
TLC
X
Column Chromatography
X
Rotoevaporation
X

Fluorescence Spectroscopy
X (revised 4/18/02)

Interactive NMR Spectra*

Compound
Benzyltriphenylphosphonium bromide
E-stilbene
meso-Stilbenedibromide
Diphenylacetylene

* In order to view these spectra you must have a program called H-NMR Viewer installed on your computer.  This program is available for free from ACD Labs.